A high-pressure study of PbCO<SUB>3</SUB> by XRD and Raman spectroscopy

ZHANG Yu-Feng; LIU Jing; QIN Zhen-Xing; LIN Chuan-Long; XIONG Lun; LI Rui; BAI Li-Gang

doi:10.1088/1674-1137/37/3/038001

Chinese Physics C> 2013, Vol. 37> Issue(3) : 038001 DOI: 10.1088/1674-1137/37/3/038001

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

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Abstract：
The pressure-induced phase transitions of PbCO₃ are studied using synchrotron radiation in a diamond anvil cell at room temperature. The XRD measurement indicates that PbCO₃ with an initial phase of aragonite-type structure undergoes two phase transitions at ～ 7.8 GPa and ～ 15.7 GPa，respectively. The higher-pressure phase appearing at ～ 15.7 GPa is stable up to 51.8 GPa. The two phase transitions are further confirmed by Raman scattering up to 23.3 GPa. During the decompression process, the high-pressure phases of PbCO₃ are gradually recovered to the starting aragonite-type structure, but exhibit some hysteresis. The bulk modulus B₀ of the aragonite-type structure is obtained to be 63± (3) GPa by fitting the volume-pressure data to the Birch-Murnaghan equation of states with B₀' fixed to 4.

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ZHANG Yu-Feng, LIU Jing, QIN Zhen-Xing, LIN Chuan-Long, XIONG Lun, LI Rui and BAI Li-Gang. A high-pressure study of PbCO₃ by XRD and Raman spectroscopy[J]. Chinese Physics C, 2013, 37(3): 038001. doi: 10.1088/1674-1137/37/3/038001

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Received: 2012-04-18
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通讯作者: 陈斌, bchen63@163.com

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沈阳化工大学材料科学与工程学院沈阳 110142

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

Corresponding author: ZHANG Yu-Feng,

Corresponding author: LIU Jing,

Received Date: 2012-04-18

Accepted Date: 2012-06-07

Available Online: 2013-03-05

Abstract: The pressure-induced phase transitions of PbCO₃ are studied using synchrotron radiation in a diamond anvil cell at room temperature. The XRD measurement indicates that PbCO₃ with an initial phase of aragonite-type structure undergoes two phase transitions at ～ 7.8 GPa and ～ 15.7 GPa，respectively. The higher-pressure phase appearing at ～ 15.7 GPa is stable up to 51.8 GPa. The two phase transitions are further confirmed by Raman scattering up to 23.3 GPa. During the decompression process, the high-pressure phases of PbCO₃ are gradually recovered to the starting aragonite-type structure, but exhibit some hysteresis. The bulk modulus B₀ of the aragonite-type structure is obtained to be 63± (3) GPa by fitting the volume-pressure data to the Birch-Murnaghan equation of states with B₀' fixed to 4.

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A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

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A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

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A high-pressure study of PbCO3 by XRD and Raman spectroscopy

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A high-pressure study of PbCO3 by XRD and Raman spectroscopy

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A high-pressure study of PbCO₃ by XRD and Raman spectroscopy

A high-pressure study of PbCO₃ by XRD and Raman spectroscopy